Domestic Distillation Tower Experimental Equipment Company

Distillation tower experimental apparatus

Stainless steel packing distillation tower experimental device model: YC-JL/T-D

Function:

1. Understand the basic structure and working principle of the experimental device for packed distillation tower;

2. Master the operation method of packed distillation tower;

3. Observe the effect of total reflux and different reflux ratios on the temperature stability of the system during distillation;

4. Master the measurement method of distillation tower efficiency.

   Main configurations:

   Tower kettle (reboiler), tower section, tower head (condenser), stainless steel θ ring packing, raw material tank, product tank, distributor, flow meter, feed pump, pipeline, valve, temperature control instrument, pressure instrument, experimental bench frame and control cabinet, etc.

   Technical Specifications:

   1. Tower kettle: with a capacity of about 8L (can also be customized according to user requirements), made of stainless steel refining, equipped with built-in electric heating tubes for heating, with a total heating power of 2 × 1000W, and has safe pressure relief and purification functions.
   2. Tower body: The entire tower is made of high-quality stainless steel material, with a tower diameter of 50mm and a packing section of ≥ 1.2m. The packing material is 304 stainless steel θ ring packing.
   3. Tower head: equipped with a tubular metal condenser, heat exchange tube diameter: 10mm, wall thickness: 1mm, heat exchange area: approximately 0.05m2.
   4. Equipped with one overhead distillate sight cup and high-temperature glass.
   5. Equipped with a raw material preheater made of stainless steel, with a heating rod power of approximately 500W.
   6. Equipped with tower top product tank and raw material tank, with a capacity of 5-10 liters, made of stainless steel material, and with automatic draining function.
   7. Temperature control system: including heating device, pressure regulating device, temperature sensor, temperature control instrument, etc. Temperature sensor: using K-type thermocouple for temperature measurement, stainless steel probe, digital display, accuracy level ± 0.1%; Temperature control instrument: 485 communication, input adopts digital calibration system, built-in commonly used thermocouple and thermal resistance nonlinear calibration table, accurate and stable measurement, the product has been tested by a third-party organization and obtained CE certification mark.
   8. Distributor: Made of refined stainless steel material, it forms a reflux ratio control system with two liquid flow meters.
   9. Feed pump: anti-corrosion magnetic drive pump, power: 30W, voltage: 220V.
   10. Device output: Taking ethanol as an example, the feed composition is 15-35%, and the composition of the top distillate is 90-95%, approximately 4L/H.
   11. The experimental console frame is made of exquisite stainless steel square tubes; The experimental desktop board and the bottom plate of the electrical control cabinet are both made of exquisite stainless steel plates. The equipment adopts a box layout design, with a compact device structure, beautiful appearance, simple process, and easy operation.
   12. Dimensions: Approximately 1300 × 500 × 2000mm. (with pulleys and locking feet)
   13. Engineering identification: including equipment tag numbers, pipeline flow arrows and markings, warning signs, and other engineering equipment concept matching.

Model of sieve plate distillation experimental device: YC-JL-D

Function:

Understand the basic structure and working principle of the sieve plate distillation tower experimental device;

1. Master the operation method of distillation tower;

2. Observe the effect of total reflux and different reflux ratios on the temperature stability of the system during distillation;

3. Master the measurement method of distillation tower efficiency.

   *Main configuration:

   Tower kettle (reboiler), tower section, tower head (condenser), tower body sight cup, fraction sight cup, preheater, raw material tank, product tank, distributor, flowmeter, feed pump, alcohol meter, pipeline, valve, temperature control instrument, pressure instrument, experimental bench frame and control cabinet, etc.

   Technical Specifications:

   *1. Tower kettle: with a capacity of 10L (can be customized according to user requirements), made of stainless steel refining, built-in electric heating tube for heating, total heating power of 2 × 1500W, automatic pressure relief, liquid level display, and natural discharge.

   2. Tower body: The entire tower is made of high-quality stainless steel material, with a diameter of 65mm and a downcomer on the tray. Number of trays: 12 pieces, with no less than 7 pieces in the distillation section. Board spacing: 80-100mm, aperture: φ 2.0mm, aperture ratio: 20%.

   *3. Tower head: equipped with a tubular stainless steel condenser, heat exchange tube diameter: 10mm, wall thickness: 1mm, heat exchange area: approximately 0.05m2.

   4. Tower body sight cup: flange connection, made of high-temperature resistant glass material;

   5. Equipped with one overhead distillate sight cup, made of high-temperature resistant glass material;

   6. Equipped with a raw material preheater, which is a stainless steel heating tank with a power of not less than 200 W;

   7. Equipped with raw material tanks and tower top product tanks, with a capacity of ≥ 10 liters, made of stainless steel material, and with automatic draining function;

   *8. Temperature control system: including heating device, pressure regulating device, temperature sensor, temperature control instrument, etc. Temperature sensor: using K-type thermocouple for temperature measurement and stainless steel probe; Temperature control instrument: digital display, accuracy level ± 0.1%, input adopts digital calibration system, built-in commonly used thermocouple and thermal resistance nonlinear calibration table, accurate and stable measurement, the product has been tested by a third-party organization and obtained CE certification mark. The temperature controller is equipped with a 485 communication interface.

   9. Pressure gauge: Range: 0-0.16MPA, Y60 pressure gauge.

   10. Distributor: Made of refined stainless steel material, it forms a reflux ratio control system with two liquid flow meters;

   11. Feed pump: Non feed pump: MP-15RM magnetic drive pump, polypropylene acid and alkali resistant pump head, flow rate: 8L/min, head: 1.5m, power: 10W, voltage: 220V.

   12. Device output: The raw material system is an ethanol water system, with a processing capacity of more than 10L/h, and the concentration of the product at the top of the tower can reach over 90%;

   13. Supporting alcohol content meter: one set of three.

   *14. The experimental console frame is made of exquisite stainless steel square tubes; The experimental bench panel and electrical control cabinet bottom plate are made of exquisite stainless steel plates, which have insulation, acid and alkali resistance, wear resistance, corrosion resistance, flame retardancy and other characteristics. The equipment adopts a box layout design, with a compact device structure, beautiful appearance, simple process, and easy operation.

   15. Dimensions: Approximately 1300 × 500 × 2200mm. (with swivel wheels and locking feet)
   16. Engineering identification: including equipment tag numbers, pipeline flow arrows and markings, warning signs, and other engineering equipment concept matching.

Experimental apparatus model for atmospheric and vacuum distillation of glass: YC-JL/B-D

Function:

Capable of performing operations such as ordinary distillation, vacuum distillation, and reactive distillation.

Work environment:

Normal and reduced pressure operation, tower temperature: within 200 ℃.

Voltage AC220V, power 2KW, standard single-phase three wire system.

Technical Specifications:

1. Glass packing tower: Tower column with a diameter of 25 × 1200mm, one unit, two feed side ports. Stainless steel θ mesh ring packing, electric heating insulation for the outer wall of the tower body (instrument temperature control/adjustable heating power).
2. Glass tower kettle, capacity 500m1, 1 unit.

3. Stainless steel heater: approximately 1.0kW, 1 unit. Temperature and reflux control at the top of the tower, independent digital display of temperature measurement at the top and bottom of the tower (instrument temperature control/adjustable heating power).

4. One tower top fully condensing glass condenser, which is a serpentine condenser with a pendulum reflux structure and serpentine condenser.

5. K-type thermocouple thermometer: 0-400 ℃, 3 pieces.

6. Temperature display instrument: temperature measurement digital display. 3 sets.

7. Voltage display and control instrument. 2 sets.

8. One reflux ratio control display instrument.

9. External control functions of one peristaltic pump: speed control, direction control, start stop control. Speed range: 0.1-100rpm. Speed resolution: 0.1rpm. Applicable hoses: 13 # 14 # 19 # 16 # 25 # 17 # 18 #. Flow range: 0.07-380mL/min.

10. The experimental console frame is made of exquisite stainless steel square tubes; The experimental bench panel and the bottom plate of the electrical control cabinet are made of exquisite stainless steel plates, which have the characteristics of durability, wear resistance, and beauty. The equipment adopts a box layout design, with a compact device structure, beautiful appearance, simple process, and easy operation.

11. Dimensions: Approximately 1200 × 550 × 2000mm. (with casters and locking feet)
12. Engineering identification: including equipment tag numbers, pipeline flow arrows and markings, warning signs, and other engineering equipment concept matching.